Thermal Behaviors of Polyamide-Layered Silicate Nanocomposites Based on 4,4'-Azodibenzoic Acid by Solution Intercalation Technique
Publish place: 1st National Conference on Nano Science and Technology
Publish Year: 1389
نوع سند: مقاله کنفرانسی
زبان: English
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شناسه ملی سند علمی:
NNTC01_080
تاریخ نمایه سازی: 8 آبان 1389
Abstract:
Two new samples of polyamide-montmorillonite reinforced nanocomposites based on 4,4'-azodibenzoic acid were prepared by a convenient solution intercalation technique. Polyamide (PA) 4 as a source of polymer matrix was synthesized by the direct polycondensation reac#on of 4,4'-azodibenzoic acid 2 with 4,4'-diamino diphenyl sulfone 3 in the presence of triphenyl phosphate (TPP), CaCl2, pyridine and N-methyl-2-pyrrolidone (NMP). Morphology and structure of the resulting PA-nanocomposite films 4a and 4b with 10 and 20% silicate particles were characterized by FTIR spectroscopy, X-ray diffraction (XRD) and scanning electron microscopy (SEM). The effect of clay dispersion and the interaction between clay and polymeric chains on the properties of nanocomposite films were investigated by using Uv-vis spectroscopy, thermogravimetric analysis(TGA) and water uptake measurements
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Authors
Meisam Shabanian
Young Researchers Club, Islamic Azad University, Arak Branch, Arak, Iran
Khalil Faghihi
Organic Polymer Research Laboratory, Department of Chemistry, Faculty of Science Arak
Mohsen Hajibeygi
Department of Chemistry, Varamin Pishva Branch, Islamic Azad University, Varamin Pishva, Iran
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