Mesoporous SiO۲-Al۲O۳: An Efficient Catalyst for Synthesis of ۴,۵-dihydro-۱,۳,۵-triphenyl-۱H-pyrazole
Publish place: Journal of Chemistry Letters، Vol: 2، Issue: 1
Publish Year: 1400
نوع سند: مقاله ژورنالی
زبان: English
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شناسه ملی سند علمی:
JR_JCHE-2-1_003
تاریخ نمایه سازی: 23 مرداد 1400
Abstract:
Mesoporous SiO۲-Al۲O۳ nano sized mixed metal oxide (MMO’s) used as a catalyst readily synthesized by hydrothermal method in high pressure autoclave. It shows highly efficient, recyclable and mild catalyst for the condensation reaction of substituted chalcone and phenyl hydrazine hydrate to obtain ۴,۵-dihydro-۱,۳,۵-triphenyl-۱H-pyrazole derivatives in excellent yields of product at short reaction times under simple experimental condition. The synthesized material particle size was controlled by CTAB as structure directing agent and calculated by BET Surface area. The structural characteristic of catalyst is identified by XRD, SEM, EDS, TEM analysis. The acidic strength of catalyst was measured by Ammonia- Temperature Programmed Desorption (NH۳-TPD).
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Authors
Deepak Tayde
M.J.M. ACS College Karanjali, Tal-Peth, Dist Nashik, Maharashtra, India. Savitribai Phule Pune University
Machhindra Lande
Department of Chemistry, Dr. Babasaheb Ambedkar Marathwada University, Aurangabad-۴۳۱۰۰۴, India