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Micro Spectrophotometric Determination and Cloud Point Extraction of Aspirin with Iron (III) in Pure Form and Pharmaceutical Drugs

عنوان مقاله: Micro Spectrophotometric Determination and Cloud Point Extraction of Aspirin with Iron (III) in Pure Form and Pharmaceutical Drugs
شناسه ملی مقاله: JR_CHM-6-7_007
منتشر شده در در سال 1401
مشخصات نویسندگان مقاله:

Noora Saad Mubder - Chemistry Department, College of Science for Women, University of Baghdad, Jadiyriah, Baghdad, Iraq
Maha Al-Tameemi - Chemistry Department, College of Science for Women, University of Baghdad, Jadiyriah, Baghdad, Iraq
Hawraa Mahmood - Chemistry Department, College of Science for Women, University of Baghdad, Jadiyriah, Baghdad, Iraq
Nahlah Kadhim Salman - Biology Department, College of Science for Women, University of Baghdad, Jadiyriah, Baghdad, Iraq
Haider Al-Neshmi - Al-Hussein Military Hospital, Baghdad, Iraq

خلاصه مقاله:
Cloud-point extraction and molecular spectrophotometry in tandem was developed and suggested as a method for detecting aspirin and iron (III) ions in pharmaceutical. In a dilute acidic medium, aspirin interacted with Fe(III) ions to produce a brightly colored [Fe(III)-aspirin] complex, which was originally as a mediated extractant, extracted into Triton X-۱۱۴ micelles, then determined by spectrophotometry at a wavelength maximum of ۵۲۷ nm. For target analytes, all experimental variables were previously adjusted to accomplish this purpose. The results showed that pre-concentration factors of ۸۰ for aspirin resulted in a detection limit of ۰.۲۳ g mL-۱ having a linear range of (۵-۱۲۰) gmL-۱ (r= ۰.۹۹۹۸). For aspirin, a mean recovery percentage of ۹۸. ± ۱.۰۹% was recorded, with precision (RSD %) ranging from ۰.۰۴-۰.۶۶ %.

کلمات کلیدی:
aspirin, Spectrophotometry, Ferric Ion, Cloud Pint Extraction

صفحه اختصاصی مقاله و دریافت فایل کامل: https://civilica.com/doc/1450535/