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Continuous flow injection analysis via NAG-۴SX۳-۳D analyzer utilized to determination of resorcinol

عنوان مقاله: Continuous flow injection analysis via NAG-۴SX۳-۳D analyzer utilized to determination of resorcinol
شناسه ملی مقاله: JR_AJGC-6-2_003
منتشر شده در در سال 1401
مشخصات نویسندگان مقاله:

Nagham Shakir Turkie - Department of chemistry, College of science, University of Baghdad, Baghdad, Iraq
Sarah Faris Hameed - Department of chemistry, College of science, University of Baghdad, Baghdad, Iraq

خلاصه مقاله:
A fast and sensitive method for detecting resorcinol by producing yellowish-green color species using the reaction of potassium dichromate with resorcinol in a sulfuric acid medium. NAG-۴SX۳-۳D analyzer was used to evaluate the transducer energy response. To improve the sensitivity of the newly developed approach, the relevant parameter was explored. The linear range (۰.۰۵-۳۲) mmol.L-۱ for resorcinol measurement and RSD percent for the repetition (n=۶) was significantly lower than ۰.۳% for (۰.۷, ۲۳ millimol.L-۱) with L.O.D.=۴۸.۱۶۸۷ ng/sample from the progressive dilution across the calibration graph's lowest concentration linear dynamic range (r=۰.۹۹۹۷), (correlation coefficient), percentage linearity (R۲ %=۹۹.۹۵). The proposed approach was compared to the previous technique (UV-spectrophotometric at λmax=۲۷۳ nm). It can be concluded that, in addition to the technique's sensitivity (developed) and the use of a few chemicals, it outperforms the ۱۰ mm irradiation of the classic reference method. Furthermore, continual dilution in CFIA enables the handling of high or low concentrations, opening up a larger range of applications. Based on the foregoing, the developed methodology is judged to be the most suited for resorcinol molecules compared to the reference techniques.

کلمات کلیدی:
Resorcinol, continuous flow injection analysis

صفحه اختصاصی مقاله و دریافت فایل کامل: https://civilica.com/doc/1472723/