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An Easy & Novel thermal Synthesis Method, characterization of MnO۲ nanoparticles

عنوان مقاله: An Easy & Novel thermal Synthesis Method, characterization of MnO۲ nanoparticles
شناسه ملی مقاله: ATEMCONF01_092
منتشر شده در نخستین همایش فناوری های نوین در انرژی و مواد در سال 1398
مشخصات نویسندگان مقاله:

KOUROSH MOTEVALLI - Department of Applied Chemistry, Faculty of Sci ence, Islamic Azad University, South Tehran Branch,Tehran, Iran
ZAHRA YAGHOUBI - IT Department, Technical& Engineering Faculty, Islamic Azad University, South Tehran Branch, Tehran, Iran
Mokhtar Panahi-Kalamuei - Young Researchers and Elites Club, South Tehran Branch,Islamic Azad University, Tehran, Iran
Majid Aliabadi - Department of Chemical Engineering, Birjand Branch,Islamic Azad University, Birjand, Iran

خلاصه مقاله:
In this paper, MnO۲ nanoparticles were very well synthesized by thermal decomposition route of manganese-metal organic framework (Mn-MOF) nanoparticles as a new manganese precursor. Mn-MOF string like nanoparticles were prepared by an easy hydrothermal method using ۱,۳,۵-benzentricarboxylic acid as organic ligand and MnCl۲. Pure cubic phase of MnO۲ nanoparticles were synthesized after calcination of Mn-MOF nanoparticless at ۲۲۵ °C for ۶h into an autoclave. The morphology and microstructure of the achieved products were characterized by X-ray diffraction patterns, energy- dispersive X-ray spectroscopy, Fourier transformed infrared spectrum, scanning electron microscopy and transition electron microscopy.

کلمات کلیدی:
synthesis, nanoparticles, thermal, string like, FTIR

صفحه اختصاصی مقاله و دریافت فایل کامل: https://civilica.com/doc/1696618/