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Preparation of Ni-microsphere using Ascorbic acid as coordinating ligandand study of its catalytic properties in sulfoxidation reactions And synthesis of۵-substituted ۱H-tetrazoles

عنوان مقاله: Preparation of Ni-microsphere using Ascorbic acid as coordinating ligandand study of its catalytic properties in sulfoxidation reactions And synthesis of۵-substituted ۱H-tetrazoles
شناسه ملی مقاله: IICC22_159
منتشر شده در بیست و دومین کنفرانس شیمی معدنی ایران در سال 1402
مشخصات نویسندگان مقاله:

Mostafa Koolivand - Department of Chemistry, Faculty of Science, Ilam University, Ilam, Iran.
Mohsen Nikoorazm - Department of Chemistry, Faculty of Science, Ilam University, Ilam, Iran.
Arash Ghorbani-Choghamarani - Department of Organic Chemistry, Bu-Ali Sina University, ۶۵۱۷۸۳۸۶۸۳, Hamedan, Iran.

خلاصه مقاله:
In this study, a novel ascorbic acid-based Ni-microsphere was prepared via thehydrothermal method. The obtained Ni-microsphere's morphology and porosity were assessedusing the following techniques: XRD, FTIR, TGA, EDS, WDX, AAS, DSC, BET, and SEM.Examining the produced MOF's catalytic activity in cyclo-condensation and sulfoxidationreactions. It was found that Recycling the Ni-microsphere five times without any loss of catalyticeffectiveness was simple.

کلمات کلیدی:
Ascorbic acid, Coordinating, ۵-substituted ۱H-tetrazoles, Oxidation reactions

صفحه اختصاصی مقاله و دریافت فایل کامل: https://civilica.com/doc/1832333/