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Title

Magnetic nanoparticle based solid phase microextraction of venlafaxine using gas chromatography – flame ionization detector (GC-FID)

Year: 1391
COI: NCOGP02_061
Language: EnglishView: 1,158
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Authors

A.H Ebrahimi Talab - Dep. of Chemistry, Faculty of Science, Islamic Azad University, Mashhad Branch, Mashhad, Iran
M Ebrahimi
S Akbari
Z Salari

Abstract:

In this paper, a fast, rapid, inexpensive, and sensitive analytical method based on nano magnetic solid phase microextraction coupled to gas chromatography–flame ionization detector (GC–FID) was developed for determination of the venlafaxine in water samples. The feasibility of employing non modified magnetic nanoparticles (MNPs), as sorbent was examined and applied to perform the extraction process. Influential parameters affecting the extraction efficiency Including pH, amount of MNPs, shaking time, and desorption condition were investigated and optimized. Under the optimized experimental conditions, a good linearity was observed in the range of 1–500 μg L−1 for the analyte, with the correlation coefficients (R2) was 0.992. The preconcentration factor of 1597 was achieved in this method. The limits of detection of the method ranged between 0.1 and 0.6 μg L−1 bases S/N=3 and Good reproducibility with the relative standard deviations (n = 5) 4.27 % were obtained. This method can be applied for environmental pollution control organizations to qualitative and quantitative analysis of environmental water samples.

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Paper COI Code

This Paper COI Code is NCOGP02_061. Also You can use the following address to link to this article. This link is permanent and is used as an article registration confirmation in the Civilica reference:

https://civilica.com/doc/202188/

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Ebrahimi Talab, A.H and Ebrahimi, M and Akbari, S and Salari, Z,1391,Magnetic nanoparticle based solid phase microextraction of venlafaxine using gas chromatography – flame ionization detector (GC-FID),2nd National Conference On Oil,Gas and petrochemicals,Gachsaran,https://civilica.com/doc/202188

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Scientometrics

The specifications of the publisher center of this Paper are as follows:
Type of center: Azad University
Paper count: 10,493
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