Extraction of Pb+2 from water samples using Amberlite resin XAD-16 impregnated with 1, 4-diaminoantraquinone
Publish place: The first national conference on environmental research
Publish Year: 1392
نوع سند: مقاله کنفرانسی
زبان: English
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شناسه ملی سند علمی:
NCER01_155
تاریخ نمایه سازی: 25 اسفند 1392
Abstract:
A simultaneous separation and pre concentration of Pb (II) ions from water samples for subsequent flame atomic absorption spectrometric determination was proposed. The procedure is based on sorption of Pb (II) at the buffering PH of 8, on a mini column(10cm length and 5mm internal diameter) filled with 0.7 g Amberlite XAD-16 resin impregnated with chelating agent of 1,4-diaminoantraquinone (DAAQ). After passing of sample solution from column, elution process was carried out with passing of 5 ml HCL 2M into column and then transferred to FAAS for determination. The sample and eluent flow rate, eluent concentration and ionic strength effect were investigated and optimized. RSD, LOD (3sb/m), recovery were fined to be 2.8%, 1.8Í10-9 M, 2.95% respectively
Keywords:
Amberlite resin XAD-16 , impregnation , 1 , 4-diaminoantraquinone , flame atomic absorption spectrometry , separation
Authors
Fatemeh Abedi
Department of Chemistry, Basic Sciences Faculty, Neyshabur Branch, Islamic Azad University, Neyshabur, Iran
Mohammad Saeid Hosseini
Department of chemisty, Basic Science Faculty, Birjand University, Birjand, Iran
Zohreh Emrani
Department of Chemistry, Basic Sciences Faculty, Neyshabur Branch, Islamic Azad University, Neyshabur, Iran