The effect of extract stevia addition on nanocrystalline SiC powder prepared by sol gel method using tetraethoxysilane as precursor
Publish place: The 6th International Conference on Exhibitiion on Metallurgy and Materials Engineering
Publish Year: 1396
نوع سند: مقاله کنفرانسی
زبان: English
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شناسه ملی سند علمی:
IMES11_121
تاریخ نمایه سازی: 7 اسفند 1396
Abstract:
Silicon carbide (SiC) Nano powder was synthesized by sol-gel method using TEOS (tetraethoxysilane) and extract stevia as precursor materials. Primary materials were mixed and then stirred with the speed of 250 rpm at 30˚C for 4 hours, the process was done at pH=4.5, Prepared solution was kept in an isolated place for 18 hours in order to finish hydrolysis reaction. Resultant gels were kept in the extraction fan for 4 hours in 60˚C to dry. In order to investigate carbothermal reduction process, samples were kept in furnace with argon atmospheres at 650, 900, 1400 and 1500˚C for 1.5, 2, 1 and 0.5 hours respectively. To remove remained Si and SiO2, pickling by HF was performed. The characterizations of the samples were performed using XRD and SEM analysis. The results shown the formation of β-SiC with the average grain size of 35 nm and spherical morphology. Increasing heating temperature from 900˚C to 1500˚C leads to an increase in the intensity of β-SiC peaks and eliminating Si and SiO2 contaminations.
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Authors
Malihe Zeraati
Malihe Zeraati: Department of Materials Science and Engineering, Shahid Bahonar University of Kerman, Kerman, Iran
Kazem Tahmasebi
Malihe Zeraati: Department of Materials Science and Engineering, Shahid Bahonar University of Kerman, Kerman, Iran