Synthesis and characterization of 4-cyano-4-[(phenylcarbothioyl)sulfanyl]pentanoic acid RAFT agent
Publish place: National Congress on Chemistry and nano-chemistry, from research to national development
Publish Year: 1396
نوع سند: مقاله کنفرانسی
زبان: English
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شناسه ملی سند علمی:
MRSS01_112
تاریخ نمایه سازی: 29 فروردین 1397
Abstract:
In this work, we used grinard reagent to prepare dithiocarboxylic acid. Then as first option, oxidation with dimethyl sulfoxide (DMSO) to diphenyldithioperoxyanhydride and its derivate was carried out. The formation of dithoesters is possible when the coupled compounds (disulfides) are allow to react with initiators such as 4,4-azobis(4-cyano pentanoic acid). The synthesized RAFT agent were identified by fourier-transform infrared (FTIR) and nuclear magnetic resonance spectroscopy(NMR).
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Authors
Alireza Hosseinzadeh
Research Laboratory of Nanopolymers, Faculty of Chemistry, University of Tabriz, Iran
Hassan Namazi
Research Laboratory of Nanopolymers, Faculty of Chemistry, University of Tabriz, Iran
Shahryar Pashaei
Department of Chemistry, Payame Noor University, Tehran, I.R of Iran
Soleyman Hosseinzadeh
Department of Chemical engineering, Payame Noor University, Tehran, I.R of Iran