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Title

Electrocatalytic multicomponent assembling of aldehydes, dimedone and 1-naphthylamine for synthesis of novel tetrahydrobenzo[c]acridin-8(7H)-one derivatives

Year: 1397
COI: JR_ICC-6-4_006
Language: EnglishView: 202
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Authors

Mohammad Reza Poor Heravi - Department of Chemistry, Payame Noor University, Abhar, Iran
Hassan Karami - Department of Chemistry, Payame Noor University, PO Box ۱۹۳۹۵-۳۶۹۷, Tehran, IRAN
Bagher Mohammadi - Department of Chemistry, Payame Noor University, PO Box ۱۹۳۹۵-۳۶۹۷, Tehran, IRAN
Vahid Azizkhani - Department of Chemistry, Payame Noor University, PO Box ۱۹۳۹۵-۳۶۹۷, Tehran, IRAN

Abstract:

An efficient and convenient synthesis of novel tetrahydrobenzo[c]acridin-8(7H)-one derivatives is described using the electrogenerated anion of acetonitriles as the base in the presence of tetrabutylammonium fluoride as an effective supporting electrolyte in a one-pot, three-component condensation of aromatic aldehyde, dimedone and 1-naphthyl amine. The reaction is carried out in an undivided cell containing an iron cathode and a graphite anode under a constant current density of 5 mA/cm2 (I=20 mA, electrode surface=5 cm2) in CH3CN at room temperature was found to be optimum for the electrochemically induced chain process and resulted in the highest yield. An efficient and convenient synthesis of novel tetrahydrobenzo[c]acridin-8(7H)-one derivatives is described using the electrogenerated anion of acetonitriles as the base in the presence of tetrabutylammonium fluoride as an effective supporting electrolyte in a one-pot, three-component condensation of aromatic aldehyde, dimedone and 1-naphthyl amine. The reaction is carried out in an undivided cell containing an iron cathode and a graphite anode under a constant current density of 5 mA/cm2 (I=20 mA, electrode surface=5 cm2) in CH3CN at room temperature was found to be optimum for the electrochemically induced chain process and resulted in the highest yield.

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Paper COI Code

This Paper COI Code is JR_ICC-6-4_006. Also You can use the following address to link to this article. This link is permanent and is used as an article registration confirmation in the Civilica reference:

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Poor Heravi, Mohammad Reza and Karami, Hassan and Mohammadi, Bagher and Azizkhani, Vahid,1397,Electrocatalytic multicomponent assembling of aldehydes, dimedone and 1-naphthylamine for synthesis of novel tetrahydrobenzo[c]acridin-8(7H)-one derivatives,https://civilica.com/doc/931356

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