Solid state synthesis of NiO nanoparticles from [(1,2-bis(2-formyl-3-methoxyphenyl)propane)nickel(II)] chloride
عنوان مقاله: Solid state synthesis of NiO nanoparticles from [(1,2-bis(2-formyl-3-methoxyphenyl)propane)nickel(II)] chloride
شناسه ملی مقاله: JR_ICC-4-3_004
منتشر شده در شماره 3 دوره 4 فصل در سال 1394
شناسه ملی مقاله: JR_ICC-4-3_004
منتشر شده در شماره 3 دوره 4 فصل در سال 1394
مشخصات نویسندگان مقاله:
Aliakbar Dehno Khalaji - Department of Chemistry, Faculty of Science, Golestan University, Gorgan, Iran
Fatemeh Gharib - Department of Chemistry, Faculty of Science, Golestan University, Gorgan, Iran
خلاصه مقاله:
Aliakbar Dehno Khalaji - Department of Chemistry, Faculty of Science, Golestan University, Gorgan, Iran
Fatemeh Gharib - Department of Chemistry, Faculty of Science, Golestan University, Gorgan, Iran
In this paper, nickel oxide (NiO) nanoparticles have been prepared by solid state thermal decomposition of an acyclic nickel(II) complex (1,2-bis(2-formyl-3-methoxyphenyl)propane)nickel(II) chloride, [NiL]Cl2, in an electrical furnace at optimal temperature, 450 ºC for 3.5 h. The nickel(II) complex is obtained via solid state synthesis using nickel(II) chloride and tetradentate O4 acyclic ligand 1,2-bis(2-formyl-3-methoxyphenyl)propane. The structure and morphology of NiO nanoparticles are characterized by Fourier transform infrared spectroscopy (FT-IR), powder X-ray diffraction (XRD), scanning electron microscopy (SEM) and transmission electron microscopy (TEM). XRD and TEM analysis show that NiO nanoparticles have pure and cubic phase with the average size of 5-10 nm.
کلمات کلیدی: Nickel oxide, nanoparticles, Solid state, nickel(II) complex
صفحه اختصاصی مقاله و دریافت فایل کامل: https://civilica.com/doc/931368/