Synthesis of Acrylonitrile Based High Internal Phase Emulsion Monoliths and their Application in Recovery of Heavy Metal Ions
Publish place: Advanced Journal of Chemistry-Section A، Vol: 3، Issue: 1
Publish Year: 1398
نوع سند: مقاله ژورنالی
زبان: English
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شناسه ملی سند علمی:
JR_AJCS-3-1_005
تاریخ نمایه سازی: 20 مهر 1398
Abstract:
Polymeric monoliths based on acrylonitrile-divinyl benzene were synthesized successfully by high internal phase emulsion (HIPE) polymerization. Highly porous polyHIPEs were prepared by variation in oil to water ratio as well as type and concentration of porogens. The porogens evaluated were toluene, chlorobenzene, heptane and chloroform. The effect of oil to water ratio and porogen type and concentrations on morphology and surface area of polyHIPEs were investigated. The polyHIPEs were modified to amidoxime functionality by treating base catalyzed reaction with hydroxylamine hydrochloride in presence of base. The treated and modified polymeric monoliths were characterized by FT-IR, SEM and surface area analysis. The modified porous polyHIPEs were tested for adsorption of Cr(VI) metal ions at various pH.
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Authors
Abdul Wasif Shaikh
Polymer Science and Engineering Division, CSIR-National Chemical Laboratory, Pune, India
Sarika Deokar
Polymer Science and Engineering Division, CSIR-National Chemical Laboratory, Pune, India
Khudbudin Mulani
Polymer Science and Engineering Division, CSIR-National Chemical Laboratory, Pune, India
Nayaku Chavan
Polymer Science and Engineering Division, CSIR-National Chemical Laboratory, Pune, India
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