Fabrication of Nb/V co-doped TiO۲ thin films and study of structural, optical and photocatalytic properties
Publish place: International Journal of Nano Dimension، Vol: 8، Issue: 3
Publish Year: 1396
نوع سند: مقاله ژورنالی
زبان: English
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JR_IJND-8-3_010
تاریخ نمایه سازی: 24 تیر 1401
Abstract:
In this study, different samples of Niobium and Vanadium co-doped titania thin films (۵-۱۰-۱۵ mol% Nb and ۵-۱۰-۱۵ mol% V) were prepared via sol−gel dip coating method, using niobium chloride as niobium precursor, ammonium metavanadate as vanadium precursor, and titanium (IV) butoxide (TBT) as titanium precursor. The effects of doping amount on the structural, optical, and photo-catalytic properties of formed thin films have been studied by X-ray diffraction (XRD), scanning electron microscopy (SEM), UV-Vis absorption and transmission electron microscopy (TEM). XRD patterns showed a decrease in peak intensities of the anatase crystalline phase by increasing the Nb/V dopant and doping inhibition effect on the grain growth, and revealed that all samples contained only anatase phase (T= ۴۷۵ ºC). The photo-catalytic activity of the thin film was measured on degradation rate of methylene blue (MB) solution under UV irradiation. Highest photo-catalytic activity of doped TiO۲ thin films were measured in the TiO۲–۵ mol% Nb-۱۵ mol% V sample (TNV۴). Small granular crystallites of ۱۰-۱۵ nm ۲D diameter were observed in electron microscope micrographs.
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Authors
Behzad Koozegar Kaleji
Department of Materials Engineering, Faculty of Engineering, Malayer University, Malayer, Iran
Navid Alami Fariman
Department of Materials Engineering, Faculty of Engineering, Malayer University, Malayer, Iran
Navid Hosseinabadi
Department of Materials Engineering and Metallurgy, Faculty of Engineering, IAU-Shiraz Branch, Shiraz, Iran
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