a new precursor for preparation of magnetite (Fe3O4) nanoparticles
Publish place: Journal of Particle Science & Technology، Vol: 1، Issue: 2
Publish Year: 1394
نوع سند: مقاله ژورنالی
زبان: English
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شناسه ملی سند علمی:
JR_JPST-1-2_001
تاریخ نمایه سازی: 26 فروردین 1397
Abstract:
An anionic Fe(II) complex, (BMIM)4[Fe(CN)6] (where BMIM is 1-butyl-3-methylimidazolium), was synthesized in ionic liquid [BMIM][PF6] under reflux condition. The complex was characterized by elemental analysis and spectroscopic methods. The magnetite (Fe3O4) nanoparticles were prepared by the hydrothermal and solvothermal (in ionic liquid [BMIM][PF6]) methods from (BMIM)4[Fe(CN)6] as a precursor. The nanoparticles were characterized by X-ray diffraction (XRD), FT-IR, and scanning electron microscopy (SEM). The results show that the preparation of magnetite using the solvothermal method in [BMIM][PF6] has more advantages over the hydrothermal method such as smaller size and higher purity.
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Authors
Mohammad Kaikhosravi
Department of Chemistry, Isfahan University of Technology, Isfahan ۸۴۱۵۶-۸۳۱۱۱, Iran
Hassan Hadadzadeh
Department of Chemistry, Isfahan University of Technology, Isfahan ۸۴۱۵۶-۸۳۱۱۱, Iran
Mohammad-Taghi Behnamfar
Department of Chemistry, Isfahan University of Technology, Isfahan ۸۴۱۵۶-۸۳۱۱۱, Iran