Synthesis and characterization of a Bi-Oxide nanoparticle ZnO/CuO by thermal decomposition of oxalate precursor method
Publish place: International Journal of Nano Dimension، Vol: 1، Issue: 1
Publish Year: 1389
نوع سند: مقاله ژورنالی
زبان: English
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شناسه ملی سند علمی:
JR_IJND-1-1_003
تاریخ نمایه سازی: 10 خرداد 1401
Abstract:
In the present work, we report the synthesis of binary nano metal oxides such as Zinc /Copper Oxide via novel dry synthetic methods such as thermal decomposition of oxalate precursor. The synthesis route involves facile solid-phase mechanochemical activation of a physical mixture of simple copper/zinc salts and oxalic acid, followed by calcination of the as-ground oxalate precursors at ۴۵۰◦C. X-ray powder diffractometry (XRD), infrared spectroscopy (FTIR), and scanning electron microscopy (SEM) were used to the thermal spectroscopic, structural, morphological characterization and surface area determination of the product respectively . An average nanocrystallite size of ۵.۰ nm was obtained for Zn/Cu, as estimated by the Scherrer’s equation.
Keywords:
Bi-Oxide , Zinc / Copper oxide , Nanoparticle , Thermal Decomposition of Oxalate Precursor Method , Chemical synthesis
Authors
M. Ghane
Department of Microbiology, Islamic Azad University Tonekabon Branch ,Tonekabon, Iran.
B. Sadeghi
Department of Chemistry, Islamic Azad University Tonekabon Branch, Tonekabon, Iran.
A.R. Jafari
Department of Microbiology, Islamic Azad University Tonekabon Branch, Tonekabon, Iran.
A.R. Paknejhad
Department of Physics, Islamic Azad University Shabestar Branch, Iran.