Solid state preparation of CdO nano-particles by thermolysis of a precursor as compacted nanosheet
Publish place: International Journal of Nano Dimension، Vol: 5، Issue: 4
Publish Year: 1393
Type: Journal paper
Language: English
View: 204
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Document National Code:
JR_IJND-5-4_013
Index date: 14 July 2022
Solid state preparation of CdO nano-particles by thermolysis of a precursor as compacted nanosheet abstract
A novel complex of cadmium (II) [CdL0.5(NO3)(H2O)](1), L= N,N-bis (O-hydroxyacetophenone) ethylene diamine, have been synthesized as single crystal and nano size. Compound 1 in nano size was obtained under sonochemical irradiation and has been characterized by IR, 1HNMR spectroscopy, X-ray powder diffraction (XRD) and scanning electron microscopy (SEM). The gray single crystal of compound 1 has been synthesized by slow evaporation and characterized by IR, 1HNMR spectroscopy. Then, Compound 1 in nano size was used as initial reagent to obtain nano-particles of cadmium (II) oxide at 673 K by direct calcination. The obtained CdO nano-particles were characterized by XRD pattern as well as SEM images.
Solid state preparation of CdO nano-particles by thermolysis of a precursor as compacted nanosheet Keywords:
Solid state preparation of CdO nano-particles by thermolysis of a precursor as compacted nanosheet authors
Z. Rashidi Ranjbar
Department of Chemistry, Shahid-Bahonar University of Kerman, Kerman, Iran. (P.O. Box ۷۶۱۶۹-۱۳۳).
I. Sheikhshoaie
Department of Chemistry, Shahid-Bahonar University of Kerman, Kerman, Iran. (P.O. Box ۷۶۱۶۹-۱۳۳).
Z. Bagheri
Department of Chemistry, Shahid-Bahonar University of Kerman, Kerman, Iran. (P.O. Box ۷۶۱۶۹-۱۳۳).