Synthesis and characterization of nano composite of minoxidil-zinc oxide
Publish place: 2nd International Conference on Composites: Characterization, Fabrication and Application
Publish Year: 1389
نوع سند: مقاله کنفرانسی
زبان: English
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شناسه ملی سند علمی:
COMPOSIT02_141
تاریخ نمایه سازی: 24 مهر 1389
Abstract:
In this study synthesis and characterization of mono dispersed spherical minoxidil-zinc oxide nano composite (1) has been performed by chemical bath method from the reaction between Zinc (II) acetate, minoxidil ligand {C9H15N5O = minoxidil = (2,4-diamino-6- piperidine-1-yl)pyrimidine N-oxide) and KI in methanol at 60 °C. Characterization of nano composite (1) was carried out by FTIR, scanning electron microscopy (SEM), EDAX and TG/DTA. The result showed that the particle size are about 77 nm. Zinc oxide nano particles was prepared from decomposition of the nano composite (1) at 400 °C. Characterization of mono dispersed spherical zinc oxide nano particles was performed by FTIR spectroscopy, scanning electron microscopy (SEM), EDAX and X-ray powder diffraction XRD. The result showed that the particle sizes are about 34 nm. Thermal analysis stablishes that zinc oxide prepared at 550 °C.
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Authors
Nasrin Shahsavan
aDepartment of Chemistry, faculty of Sciences, Shahreray Azad University
Maryam Ranjbar
Department of Chemical Industry ,Iranian Research Organization for Science and Technology
Mohammad Yousefi
Department of Chemistry, faculty of Sciences, Shahreray Azad University
S.Heydar Mahmodi Najafi
Department of Chemical Industry ,Iranian Research Organization for Science and Technology
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