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Title

Analytical Methods: Electrochemical azido-selenenylation of some olefins by cyclic voltammetry and controlled-potential coulometry

فصلنامه روش های تجزیه در شیمی محیط زیست، دوره: 1، شماره: 1
Year: 1398
COI: JR_AMECJ-1-1_008
Language: EnglishView: 168
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Authors

ahmad rouhollahi - Chemistry Department, Faculty of Science, K.N. Toosi University of Technology, Tehran ۱۵۴۱۸, Iran.
zeenat asghari - Chemistry Department, Faculty of Science, K.N. Toosi University of Technology, Tehran ۱۵۴۱۸, Iran.
barahman movassagh - Chemistry Department, Faculty of Science, K.N. Toosi University of Technology, Tehran ۱۵۴۱۸, Iran.

Abstract:

Electrochemical azido-phenylselenenylation of some olefins was studied with the oxidation of diphenyl diselenide in the presence of some olefins and sodium azide in dimethyl formamide containing tetra butyl ammonium perchlorate as supporting electrolyte in an H-type cell. The electrochemical oxidation of the mixture of (PhSe)2, olefins, and NaN3 was studied by cyclic voltammetry and controlled-potential coulometry. Anti product can be obtained with Markovnikov orientation. This product was characterized .by 1H, 13C NMR, and IR spectroscopy

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rouhollahi, ahmad and asghari, zeenat and movassagh, barahman,1398,Analytical Methods: Electrochemical azido-selenenylation of some olefins by cyclic voltammetry and controlled-potential coulometry,https://civilica.com/doc/991028

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