Catalyst-Free One-Pot Four-Component Synthesis of ۳-(Imino)-pyrrolo[۲,۱-a]isoquinolines in Glycerol: Two Different Products through Two Different Purification Methods

Catalyst-Free One-Pot Four-Component Synthesis of 3-(Imino)-pyrrolo[2,1-a]isoquinolines in Glycerol: Two Different Products through Two Different Purification Methods abstract

The one-pot four component synthesis of 3-(Imino)-2,3-dihydropyrrolo[2,1-a]isoquinoline-1,1(10bH)-dicarbonitrile derivatives via a catalyst-free reaction between aryl aldehydes, malononitrile, isoquinoline and isocyanides was successfully conducted in glycerol as a benign, nontoxic and biodegradable promoting reaction medium. The progress of the reaction with two different common purification methods were investigated. Moreover, synthesized products were examined as chemical sensors for the detection of a wide range of metal ions and it was successful for the detection of Co2+ ions.

Catalyst-Free One-Pot Four-Component Synthesis of 3-(Imino)-pyrrolo[2,1-a]isoquinolines in Glycerol: Two Different Products through Two Different Purification Methods Keywords:

Multicomponent synthesis , In column chromatography reaction , Glycerol , Sustainable reaction medium , Isocyanide

Catalyst-Free One-Pot Four-Component Synthesis of 3-(Imino)-pyrrolo[2,1-a]isoquinolines in Glycerol: Two Different Products through Two Different Purification Methods authors

Seyed Ali Jehbez

Department of Applied Chemistry, Shiraz Branch, Islamic Azad University, P.O. Box ۷۱۹۹۳-۵, Shiraz, Iran

Hamidreza Safaei

Department of Applied Chemistry, Shiraz Branch, Islamic Azad University, P.O. Box ۷۱۹۹۳-۵, Shiraz, Iran

Mohsen Shekouhy

Chemistry Department, College of Sciences, Shiraz University, Shiraz, Iran

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Link to this Paper:

https://civilica.com/doc/1766141

Document National Code:

JR_ORGC-6-1_002

Index date: 25 September 2023

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Jehbez, Seyed Ali and Safaei, Hamidreza and Shekouhy, Mohsen,1399,Catalyst-Free One-Pot Four-Component Synthesis of 3-(Imino)-pyrrolo[2,1-a]isoquinolines in Glycerol: Two Different Products through Two Different Purification Methods,https://civilica.com/doc/1766141

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The specifications of the publisher center of this Paper are as follows:

Ranking of Islamic Azad University of Shiraz

Type of center: دانشگاه آزاد

Paper count: 11,382

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